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19 08 2021 Here we show that using solvent less methods such as ball milling enabled the production of the hexapeptide Boc Ala Phe Gly 2 OBn at the gram scale with high overall yield 77 5 linear steps This is the longest peptide chain synthesized in a ball mill to date in which the amino acid sequence is precisely controlled.
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Click to chatIn this study ball milling was performed on Fe 10 Y2O3 5 Ti powders for different times without adding a process control agent Heat treatment was then applied at 900 to 1200 °C.
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Click to chatA mechanical ball milling method for ultrafast synthesis of a nickel based metal organic framework Ni MOF has been proposed The Ni MOF was successfully synthesized in merely one minute without any solvent additives or preliminary preparation The effect of milling time mechano frequency type of assistant liquid and amount of assistant water were systematically explored.
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Click to chat15 07 2021 After milling for 6 h all other peaks of the Cr phase disappeared except for a broad peak of 110 With further milling to 10 h the 110 peak of the Cr phase disappeared during plasma milling but it was still detected during conventional milling The results indicate that the W–Cr mixtures experienced some phase change during ball milling.
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